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1 article(s) from Fischer, Roland C

Simple activation by acid of latent Ru-NHC-based metathesis initiators bearing 8-quinolinolate co-ligands

Julia Wappel,
Roland C. Fischer,
Luigi Cavallo,
Christian Slugovc and
Albert Poater

Beilstein J. Org. Chem. 2016, 12, 154–165, doi:10.3762/bjoc.12.17

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Scheme 1: Synthesis of 1-4; only the isolated and characterized complexes are shown.

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Figure 1: Solid state structure of complexes 2a and 2b as retrieved from single crystal X-ray diffraction.

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Figure 2: Time/conversion plot for the polymerization of 5 by preinitiators 1–4 in the presence of HCl ([5]:[...

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Figure 3: ¹H NMR spectrum in the low-field region of the active species for complexes 4 and M32.

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Scheme 2: Energetics of 2a and 2b protonation in kcal/mol.

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Figure 4: Reaction pathway of the transformation of 2b to HovII (energies in kcal/mol; main distances in Å).

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Figure 5: DTA-TGA measurements for polymerizations of DCPD with catalysts 1b and 2b; Reaction conditions: [ca...

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Published 28 Jan 2016

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